FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2000660505> ?p ?o ?g. }

• W2000660505 endingPage "214" @default.
• W2000660505 startingPage "209" @default.
• W2000660505 abstract "A headspace solid-phase dynamic extraction (HS-SPDE) technique was developed by the use of polypyrrole (PPy) sorbent, electropolymerized inside the surface of a needle, as a possible alternative to solid-phase microextraction (SPME). Thermal desorption was subsequently, employed to transfer the extracted analytes into the injection port of a gas chromatography–mass spectrometry (GC–MS). The PPy sorbent including polypyrrole-dodecyl sulfate (PPy-DS) was deposited on the interior surface of a stainless steel needle from the corresponding aqueous electrolyte by applying a constant deposition potential. The homogeneity and the porous surface structure of the coating were examined using the scanning electron microscopy (SEM). The developed method was applied to the trace level extraction of some polycyclic aromatic hydrocarbons (PAHs) from aqueous sample. In order to enhance the extraction efficiency and increase the partition coefficient of analytes, the stainless steel needle was cooled at 5 °C, while the sample solution was kept at 80 °C. Optimization of influential experimental conditions including the voltage of power supply, the time of PPy electrodeposition, the extraction temperature, the ionic strength and the extraction time were also investigated. The detection limits of the method under optimized conditions were in the range of 0.002–0.01 ng mL−1. The relative standard deviations (R.S.D.) at a concentration level of 0.1 ng mL−1 were obtained between 7.54 and 11.4% (n = 6). The calibration curves of PAHs showed linearity in the range of 0.01–10 ng mL−1. The proposed method was successfully applied to the extraction of some selected PAHs from real-life water samples and the relative recoveries were higher than 90% for all the analytes." @default.
• W2000660505 created "2016-06-24" @default.
• W2000660505 creator A5014535107 @default.
• W2000660505 creator A5057913220 @default.
• W2000660505 creator A5087000678 @default.
• W2000660505 date "2009-02-01" @default.
• W2000660505 modified "2023-09-26" @default.
• W2000660505 title "An interior needle electropolymerized pyrrole-based coating for headspace solid-phase dynamic extraction" @default.
• W2000660505 cites W122154721 @default.
• W2000660505 cites W1486909458 @default.
• W2000660505 cites W1594409634 @default.
• W2000660505 cites W1968596206 @default.
• W2000660505 cites W1976894603 @default.
• W2000660505 cites W1978071818 @default.
• W2000660505 cites W1988008903 @default.
• W2000660505 cites W1993623000 @default.
• W2000660505 cites W2000837912 @default.
• W2000660505 cites W2002223284 @default.
• W2000660505 cites W2022601115 @default.
• W2000660505 cites W2029910146 @default.
• W2000660505 cites W2037866782 @default.
• W2000660505 cites W2039338285 @default.
• W2000660505 cites W2039536486 @default.
• W2000660505 cites W2049898411 @default.
• W2000660505 cites W2066720030 @default.
• W2000660505 cites W2083801266 @default.
• W2000660505 cites W2093370185 @default.
• W2000660505 cites W2111274003 @default.
• W2000660505 cites W2152851766 @default.
• W2000660505 doi "https://doi.org/10.1016/j.aca.2008.12.047" @default.
• W2000660505 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/19185122" @default.
• W2000660505 hasPublicationYear "2009" @default.
• W2000660505 type Work @default.
• W2000660505 sameAs 2000660505 @default.
• W2000660505 citedByCount "45" @default.
• W2000660505 countsByYear W20006605052012 @default.
• W2000660505 countsByYear W20006605052013 @default.
• W2000660505 countsByYear W20006605052014 @default.
• W2000660505 countsByYear W20006605052015 @default.
• W2000660505 countsByYear W20006605052016 @default.
• W2000660505 countsByYear W20006605052017 @default.
• W2000660505 countsByYear W20006605052018 @default.
• W2000660505 countsByYear W20006605052020 @default.
• W2000660505 countsByYear W20006605052021 @default.
• W2000660505 crossrefType "journal-article" @default.
• W2000660505 hasAuthorship W2000660505A5014535107 @default.
• W2000660505 hasAuthorship W2000660505A5057913220 @default.
• W2000660505 hasAuthorship W2000660505A5087000678 @default.
• W2000660505 hasConcept C113196181 @default.
• W2000660505 hasConcept C119128265 @default.
• W2000660505 hasConcept C147789679 @default.
• W2000660505 hasConcept C150394285 @default.
• W2000660505 hasConcept C162356407 @default.
• W2000660505 hasConcept C17525397 @default.
• W2000660505 hasConcept C178790620 @default.
• W2000660505 hasConcept C184651966 @default.
• W2000660505 hasConcept C185592680 @default.
• W2000660505 hasConcept C205345274 @default.
• W2000660505 hasConcept C23531484 @default.
• W2000660505 hasConcept C2777232022 @default.
• W2000660505 hasConcept C2777899863 @default.
• W2000660505 hasConcept C2778533135 @default.
• W2000660505 hasConcept C43617362 @default.
• W2000660505 hasConcept C4725764 @default.
• W2000660505 hasConcept C52859227 @default.
• W2000660505 hasConcept C81426234 @default.
• W2000660505 hasConceptScore W2000660505C113196181 @default.
• W2000660505 hasConceptScore W2000660505C119128265 @default.
• W2000660505 hasConceptScore W2000660505C147789679 @default.
• W2000660505 hasConceptScore W2000660505C150394285 @default.
• W2000660505 hasConceptScore W2000660505C162356407 @default.
• W2000660505 hasConceptScore W2000660505C17525397 @default.
• W2000660505 hasConceptScore W2000660505C178790620 @default.
• W2000660505 hasConceptScore W2000660505C184651966 @default.
• W2000660505 hasConceptScore W2000660505C185592680 @default.
• W2000660505 hasConceptScore W2000660505C205345274 @default.
• W2000660505 hasConceptScore W2000660505C23531484 @default.
• W2000660505 hasConceptScore W2000660505C2777232022 @default.
• W2000660505 hasConceptScore W2000660505C2777899863 @default.
• W2000660505 hasConceptScore W2000660505C2778533135 @default.
• W2000660505 hasConceptScore W2000660505C43617362 @default.
• W2000660505 hasConceptScore W2000660505C4725764 @default.
• W2000660505 hasConceptScore W2000660505C52859227 @default.
• W2000660505 hasConceptScore W2000660505C81426234 @default.
• W2000660505 hasIssue "2" @default.
• W2000660505 hasLocation W20006605051 @default.
• W2000660505 hasLocation W20006605052 @default.
• W2000660505 hasOpenAccess W2000660505 @default.
• W2000660505 hasPrimaryLocation W20006605051 @default.
• W2000660505 hasRelatedWork W2000935814 @default.
• W2000660505 hasRelatedWork W2023492373 @default.
• W2000660505 hasRelatedWork W2048528605 @default.
• W2000660505 hasRelatedWork W2170176786 @default.
• W2000660505 hasRelatedWork W2762971075 @default.
• W2000660505 hasRelatedWork W2802927235 @default.
• W2000660505 hasRelatedWork W3083689796 @default.
• W2000660505 hasRelatedWork W4283392280 @default.
• W2000660505 hasRelatedWork W4384937350 @default.

• next