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• W2000666013 abstract "This paper presents two sample treatments, dispersive liquid–liquid microextraction (DLLME) and QuEChERS for the determination of 9 sulfonamides, regulated by the EU Council in milk samples. Both methods represent useful alternatives to conventional procedures based mainly in solid-phase extraction, in terms of simplicity, reduction of organic solvents, sample throughput and effectiveness for cleaning-up complex samples. They have been evaluated and compared in terms of efficiency, trueness, sensitivity and precision, using HPLC with fluorescence detection employing a previous derivatisation step with fluorescamine. Clean extracts were obtained with recoveries between 90.8–104.7% and 83.6–104.8% for DLLME and QuEChERS, respectively. Matrix-matched calibration curves were established for both methods using milk samples spiked at four concentration levels. LODs (3xS/N) lower than 1.21 μg L−1 and 2.73 μg L−1 for DLLME and QuEChERS, respectively, were obtained in all cases. The precision, in terms of repeatability and intermediate precision, was lower than 10% in all cases." @default.
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• W2000666013 date "2014-01-01" @default.
• W2000666013 modified "2023-10-18" @default.
• W2000666013 title "Alternative sample treatments for the determination of sulfonamides in milk by HPLC with fluorescence detection" @default.
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• W2000666013 doi "https://doi.org/10.1016/j.foodchem.2013.08.008" @default.
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