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• W2000688288 abstract "Magic angle spinning and 14N irradiation have been employed to perturb the 14N spin bath, in a new spin-echo triple resonance solid-state NMR experiment. Spinning introduces a time dependence in the 14N quadrupolar interaction, permitting transitions between the three |I, m〉 states, two or four times per rotor cycle; this alters the evolution of a 14N-coupled 13C spin. The reduction in 13C echo intensity, on 14N irradiation during the echo period, is greater for shorter CN distances. Irradiation at a constant frequency is more effective than sweeping through the 14N resonance. 14N double-quantum spectra are obtained indirectly by irradiation of the double-quantum transition." @default.
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• W2000688288 date "1992-05-01" @default.
• W2000688288 modified "2023-09-29" @default.
• W2000688288 title "The detection of weak heteronuclear coupling between spin 1 and spin nuclei in MAS NMR; 14N/13C/1H triple resonance experiments" @default.
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• W2000688288 doi "https://doi.org/10.1016/0009-2614(92)85486-t" @default.
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