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• W2000692227 abstract "The co-ordination abilities of 2,5,8-trithia[9]-o-benzenophane (L1) are compared with several S3-crown macrocycles by structural, spectral and electrochemical techniques. Ligand L1 shows intermediate behaviour relative to the well known ligands 1,4,7-trithiacyclononane and 1,5,9-trithiacyclododecane. The synthesis and characterization of CuII, CuI, NiII and CoII complexes with L1 are carried out. Crystal and molecular structures of two complexes are determined: [CuL1(Cl)], monoclinic, space group P21/a, a= 13.562(6), b= 8.046(1), c= 13.770(6)Å, β= 109.96(2)°, Z= 4, R= 0.041 and R′= 0.045; [NiL21][BF4]2, monoclinic, space group P21/c, a= 9.430(2), b= 14.879(2), c= 11.451(2)Å, β= 113.59(1)°, Z= 2, R= 0.058 and R′= 0.057." @default.
• W2000692227 created "2016-06-24" @default.
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• W2000692227 date "1993-01-01" @default.
• W2000692227 modified "2023-09-26" @default.
• W2000692227 title "Co-ordination of the crown thioether 2,5,8-trithia[9]-o-benzenophane (L1). Synthesis and crystal structures of [CuL1(CI)] and [NiL12][BF4]2" @default.
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• W2000692227 doi "https://doi.org/10.1039/dt9930002969" @default.
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