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- W2000692778 abstract "A new ion exclusion HPLC procedure accomplished with a pulsed electrochemical detection for the determination of several common aliphatic acids is described. A triple-step waveform of the applied potentials, based on the formation/inhibition of PtOH species on the electrode surface, is successfully used for sensitive detection of several aliphatic acids in flowing systems avoiding pre- or postcolumn derivatization and/or cleanup procedures. Under optimal chromatographic conditions (i.e., 50 mM HClO4) the proposed method allowed detection limits between 0.5 and 7 μM for all investigated acids, and the dynamic linear range spanned generally over 1 or 2 orders of magnitude. Determination of citric, malic, tartaric, lactic, formic, and acetic acids in several foods and beverages was performed, in ∼15 min, without the necessity of any sample pretreatment. Keywords: Electrochemical detection; chromatography; aliphatic acids; food analysis" @default.
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- W2000692778 date "2001-11-17" @default.
- W2000692778 modified "2023-09-27" @default.
- W2000692778 title "Determination of Aliphatic Organic Acids by High-Performance Liquid Chromatography with Pulsed Electrochemical Detection" @default.
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- W2000692778 doi "https://doi.org/10.1021/jf010557d" @default.
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