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- W2000703223 abstract "A rapid and economical method for the determination in meat of androgens, estrogens, progestogens and corticoids, including some precursors and metabolites, has been developed. The extracted steroids are separated in a polar, a neutral, and a phenolic fraction by C8-SPE followed by a liquid–liquid extraction of the phenolates. Each fraction is separately purified by normal-phase SPE. The different steroid fractions can be analysed either together to obtain a comprehensive hormone pattern in one step or separately to enhance detection selectivity and sensitivity. Using a universally applicable silylation of the hydroxyl and keto groups, detection limits of 0.02–0.1 μg/kg are reached by GC–MS (EI) in the selected ion monitoring mode." @default.
- W2000703223 created "2016-06-24" @default.
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- W2000703223 date "1997-12-01" @default.
- W2000703223 modified "2023-10-10" @default.
- W2000703223 title "Simultaneous determination of anabolic and catabolic steroid hormones in meat by gas chromatography–mass spectrometry" @default.
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- W2000703223 doi "https://doi.org/10.1016/s0378-4347(97)00460-x" @default.
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