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• W2000710792 abstract "Abstract The original synthesis and stereochemical characterization of the [Pd12(μ3-I)2(μ4-I)3(μ2-CO)6L6]+ monocation (1) (L = PEt3; [PF6]− salt) was an outgrowth of our investigation of the chemical behavior of two unusual thallium–palladium clusters: (μ6-Tl)[Pd3(CO)3L3]2+ (2) which possesses a Pd3TlPd3 sandwich framework, and [Tl2Pd12(CO)9L9]2+ (3) which may be viewed as edge-fusions of three Pd5 trigonal bipyramids to a central Tl2Pd3 trigonal bipyramid. Room-temperature reactions of 2 and 3 with I2 in THF gave rise in each case to small yields ( ( NBu 4 n ) ( PF 6 ) . The square-planar palladium(II) geometries of the iodide-bridged dimeric 7 and monomeric 8 are compared with each other and with those of the previous crystallographically determined 8 (at room temperature) and several crystallographically known analogues (with different phosphine ligands); corresponding molecular parameters were found to be in remarkably close agreement with distinct bond-length variations in bridging Pd–I(b) and terminal Pd–P bonds being readily attributed to the well-documented trans influence." @default.
• W2000710792 created "2016-06-24" @default.
• W2000710792 creator A5017470156 @default.
• W2000710792 creator A5026095654 @default.
• W2000710792 date "2005-03-01" @default.
• W2000710792 modified "2023-09-26" @default.
• W2000710792 title "First high-nuclearity palladium halide/carbonyl/phosphine cluster, [Pd12(μ3-I)2(μ4-I)3(μ2-CO)6(PEt3)6]+ monocation containing an octacapped octahedral Pd6(μ3-Pd)6(μ3-I)2 fragment: structure-to-synthesis generation from different synthetic routes" @default.
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• W2000710792 doi "https://doi.org/10.1016/j.ica.2004.09.064" @default.
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