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- W2000712437 abstract "Abstract The crystal structures of 1,2- O -( S )-(1-aminomethylethylidene)-α- d -glucopyranose ( 1 ) and 1,2- O -( R )-(1- tert -butoxyethylidene)-α- d -glucopyranose ( 2 ) have been analysed by X-ray diffraction methods. The pyranoid rings in 1 and 2 have flattened 4 C 1 conformations, the dioxolane ring in 1 has a half-chair 1 T O-1 conformation, and that in 2 a 2 T O-2 conformation distorted towards 2 E . The 1 H-n.m.r. spectra of 1 and 2 have been analysed by computer simulation. The computed best values of the vicinal coupling constants and the n.O.e. measurements can be interpreted in terms of a preponderant, distorted 4 C 1 conformation in solution, although long-range H,H coupling and low-temperature 13 C-n.m.r. spectra suggest the presence of a conformational equilibrium." @default.
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- W2000712437 date "1985-06-01" @default.
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- W2000712437 title "Conformation of 1,2-O-(S)-(1-aminomethylethylidene)-α-d-glucopyranose and 1,2-O-(R)-(1-tert-butoxyethylidene)-α-d-glucopyranose" @default.
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- W2000712437 doi "https://doi.org/10.1016/0008-6215(85)90007-2" @default.
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