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- W2000715955 abstract "Abstract The formation of the gas-phase non-covalent complexes of diclofenac sodium with cyclodextrins (CDs) was studied by electrospray ionization/time-of-flight mass spectrometry (ESI/TOFMS). The continuous variation method was utilized to elucidate the stoichiometry. Mass spectrums revealed the stoichiometric ratios of complexes with 1:1, 2:1, 3:1 and 1:2 (β-cyclodextrin:diclofenac sodium) in deionized water or ethanol. The influence of cavity size of CD and the pH values of solution on the mixture system were investigated in detail. Only one complex peak was observed in α-CD, which is different from β- and γ-CD. These results demonstrated that ESI/TOFMS is a complementary technique for study of the non-covalent complex. Keywords: CyclodextrinsDiclofenac sodiumElectrospray ionization/time-of-flightStoichiometric ratio Acknowledgments This research work was supported by the National Natural Science Foundation of China (No. 20175034), and by Natural Science Foundation of Shanghai (No. 00ZA14077)." @default.
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- W2000715955 date "2003-01-04" @default.
- W2000715955 modified "2023-10-07" @default.
- W2000715955 title "The Determination of Non-covalent Complexes of Diclofenac Sodium and Cyclodextrins by Electrospray Ionization/Time-of-Flight Mass Spectrometry" @default.
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- W2000715955 doi "https://doi.org/10.1081/al-120017705" @default.
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