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- W2000732671 abstract "The helix–coil transition of poly-N5-(3-hydroxypropyl)-L-glutamine (PHPLG) has been studied in methanol–water by CD and cmr spectroscopy. For polydisperse PHPLG, two separate peaks arising from residues in helical and random-coil conformations are observed during the transition for both main-chain carbons. These results are discussed and compared to those observed in the case of a polymer sample obtained by racemization of PHPLG in 0.1 M NaOH and of PHPLG samples of controlled molecular weight and dispersity. The dominant influence of the molecular-weight heterogeneity on the double-peak phenomenon has been verified. The linewidths and chemical shift of the 13C resonances are discussed in terms of side-chain–main-chain interactions and side-chain solvation." @default.
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- W2000732671 date "1974-11-01" @default.
- W2000732671 modified "2023-09-25" @default.
- W2000732671 title "Conformational behavior of poly-N5-(3-hydroxypropyl)-L-glutamine in water-methanol mixtures studied by13C nmr and CD spectroscopy" @default.
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- W2000732671 doi "https://doi.org/10.1002/bip.1974.360131105" @default.
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