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- W2000735234 abstract "Abstract Our synthesis work on the insect antifeedant azadirachtin is described. Particular emphasis is placed on the key coupling of a left-hand decalin fragment with a right-hand hydroxydihydrofuran acetal unit via a Claisen rearrangement reaction of an intermediate propargylic enol ether. New chemistry has been developed leading to control of an endo -selective intramolecular Diels–Alder reaction using silicon, which was essential for the construction of the appropriately functionalized decalin fragment. In order to install the five-ring hemiacetal of azadirachtin, we also developed a new ring contraction protocol via an intermediate six-ring cyano ester." @default.
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- W2000735234 date "2005-01-01" @default.
- W2000735234 modified "2023-09-23" @default.
- W2000735234 title "Development of methods suitable for natural product synthesis: The azadirachtin story" @default.
- W2000735234 doi "https://doi.org/10.1351/pac200577071115" @default.
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