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- W2000737244 abstract "Abstract Chemical vapor transport of platinum (Pt) and rhodium (Rh) has been studied in closed ampoules using a 900–800 °C over 100 mm gradient for periods of 123–365 days. The ability of O 2 , air, and H 2 O to act as transport agents has been evaluated, control experiments have been performed with vacuum, N 2 , and Ar, and surveying experiments have been made with NH 3 , NO, and H 2 . Transport of Pt and Rh occurs in the presence of oxygen (regardless of source), manifested as single-crystal growth at the colder end of the ampoules. PtO 2 and RhO 2 were identified as vapor molecules by in situ mass spectrometric monitoring. A small transport of Rh is indicated for H 2 O as agent, whereas no transport is observed in N 2 , H 2 , NH 3 , and Ar atmospheres." @default.
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- W2000737244 date "2005-05-01" @default.
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- W2000737244 title "Chemical vapor transport of platinum and rhodium with oxygen as transport agent" @default.
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- W2000737244 doi "https://doi.org/10.1016/j.jcrysgro.2005.02.024" @default.
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