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- W2000763971 abstract "A new tetradentate tetraaza ligand was prepared via Schiff-base condensation of 3,4-diaminotoluene with 2,3-butandione monoxime in aqueous solution. This ligand coordinates cobalt(III) through nitrogen donors in equatorial positions with loss of one oxime proton with concomitant formation of an intramolecular hydrogen bond. A series of cobalt(III) complexes, [CoLX2] (X = Cl−, Br−, or I−), [SCNCoLBr], [CNCoLBr], [BF2CoLBr], and [YCoLBr]ClO4 (Y = pyridine, thiophene, triphenylphosphine, or n-pentylamine), was synthesized. The compounds were characterized based on the elemental analysis (C, H, N), electrical conductance, magnetic moment measurements, and spectral studies (IR, 1H NMR, and UV-Vis). Thermal stabilities of representative complexes were examined by using thermal analysis (TGA and DTG). The reported complexes are d6 low-spin diamagnetic and a distorted octahedral environment was proposed. All complexes undergo tetragonal distortion as evidenced by splitting of 1T1g and 1T2g levels of the pseudo-oc..." @default.
- W2000763971 created "2016-06-24" @default.
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- W2000763971 date "2011-09-23" @default.
- W2000763971 modified "2023-10-16" @default.
- W2000763971 title "Synthesis, characterization, and ascorbic acid oxidase biomimetic catalytic activity of cobalt(III) oxime complexes" @default.
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- W2000763971 doi "https://doi.org/10.1080/00958972.2011.621166" @default.
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