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• W2000790535 abstract "Phenylated cyclopentasilanes Si5Ph10−nXn with X = OSO2CF3, F, Cl, Br, I or H and n = 1 or 2 were prepared in high yield by dearylation of Si5Ph10 with trifluoremethanesulphonic acid (CF3SO3H) and subsequent reaction with lithium or potassium halides and LiAlH4. The trans-1,3-isomers of Si5Ph8X2 were isolated by crystallization and the crystal structure of trans-1,3-difluorooctaphenyl-cyclopentasilane was determined. cis-1,3-, trans-1,2- and cis-1,2-Si5Ph8X2 were identified and characterized by 1H, 19F and 29Si NMR spectroscopy. SiSi coupling constants were measured using INADEQUATE pulse sequences." @default.
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• W2000790535 date "1996-01-01" @default.
• W2000790535 modified "2023-09-24" @default.
• W2000790535 title "Synthesis, spectroscopy and structure of phenylated cyclopentasilanes" @default.
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• W2000790535 doi "https://doi.org/10.1016/0022-328x(95)05675-f" @default.
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