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- W2000807178 abstract "Abstract The crystallization behavior of poly(e-caprolactone) (PCL) homopolymers and PCL blocks confined in identical lamellar nanodomains (L-domains) has been examined using differential scanning calorimetry and synchrotron small-angle X-ray scattering as a function of PCL layer thickness d and crystallization temperature. The PCL homopolymers confined in the L-domains with d = 8.7 nm (small L-domain) and 15.8 nm (large L-domain) were prepared using microphase separation of PCL- block -polystyrene (PCL- b -PS) copolymers with a photocleavable o -nitrobenzyl group (ONB) between PCL and PS blocks, followed by the photocleavage of ONB with UV-irradiation. The PCL crystallinity showed a conventional sigmoidal evolution both for PCL blocks and PCL homopolymers confined in the large L-domain. However, it increased monotonously with no induction time for PCL blocks but sigmoidally for PCL homopolymers confined in the small L-domain. The substantial differences in crystallization mechanism between PCL blocks and PCL homopolymers confined in the small L-domain are discussed on the basis of chain mobility during crystallization." @default.
- W2000807178 created "2016-06-24" @default.
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- W2000807178 date "2014-08-01" @default.
- W2000807178 modified "2023-10-06" @default.
- W2000807178 title "Crystallization behavior of poly(ε-caprolactone) chains confined in lamellar nanodomains" @default.
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- W2000807178 doi "https://doi.org/10.1016/j.polymer.2014.06.049" @default.
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