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- W2000815262 endingPage "2094" @default.
- W2000815262 startingPage "2089" @default.
- W2000815262 abstract "Aus Gemengen von LnOCl, LnCl3 und GeO2 (2:1:1) wurden durch Erhitzen in evakuierten Quarzglasampullen (eingelegte Pt-Hülsen) die Verbindungen Ln3GeO4Cl5 (Ln = LaNd) dargestellt. Die Notwendigkeit, die Darstellungstemperaturen in der Reihe Ln = LaNd herabzusetzen (La: T = 900°C, 8 d; Ce: T = 800°C, 9d; Pr, Nd: T = 650°C, 13 d), deutet auf eine in dieser Richtung abnehmende thermodynamische Stabilität hin. Die Verbindung La3VO4Cl5 wurde aus einem Gemenge (2:1:1) von LaOCl, LaCl3 und VO2 erhalten (900°C, 8d) und elektronenmikroskopisch untersucht. Preparation and Electronmicroscopic Investigation of New Compounds Ln3MO4Cl5 (Ln = LaNd; M = Ge, V) By heating mixtures of LnOCl, LnCl3 und GeO2 (2:1:1) in evacuated silica tubes (Pt-shells inside) the compounds Ln3GeO4Cl5 (Ln = LaNd) were prepared. The case that the temperature of preparation (La: T = 900°C, 8d; Ce: T = 800°C, 9d; Pr, Nd: T = 650°C, 13 d) had to be reduced from Ln = La to Ln = Nd indicates a decreasing thermodynamic stability in this direction. The compound La3VO4Cl5 was prepared by heating (900°C, 8d) a mixture (2:1:1) of LaOCl, LaCl3 and VO2 and was investigated by electronmicroscopic techniques." @default.
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- W2000815262 date "1996-12-01" @default.
- W2000815262 modified "2023-10-08" @default.
- W2000815262 title "Darstellung und elektronenmikroskopische Untersuchung neuer Verbindungen des Typs Ln3MO4Cl5 (Ln = La?Nd; M = Ge, V)" @default.
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- W2000815262 doi "https://doi.org/10.1002/zaac.19966221216" @default.
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