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• W2000822030 abstract "Equimolar quantities of [MoX(CO)2(NCMe)2(η3-C3H4R)] (X=Cl, R=H or Me; X=Br, R=H) and [MI2(CO)3{MeC(CH2PPh2)3-P,P′}] (M=Mo or W) react in CH2Cl2 at room temperature to eventually give the tetrametallic complexes, [{Mo(μ-X)(CO)2(LMo or LW)(η3-C3H4R)}2] {LMo=[MoI2(CO)3{MeC(CH2PPh2)3-P,P′}]; LW=[WI2(CO)3{MeC(CH2PPh2)3-P,P′}]} (1–6) in good yield. Reaction of [MoX(CO)2(NCMe)2(η3-C3H4R)] (X=Cl, R=H or Me; X=Br, R=H) with 2 equiv. of LMo or LW affords the trimetallic complexes [MoX(CO)2(LMo or LW)2(η3-C3H4R)] (7–12). Treatment of [Fe2(CO)9] with 2 equiv. of LMo or LW in CH2Cl2 at room temperature yields the bimetallic complexes, [Fe(CO)4(LMo or LW)] (13 and 14). Equimolar amounts of [FeI(CO)2(Cp or Cp′)] (Cp=C5H5; Cp′=C5H4Me) and LMo or LW react in warm CH2Cl2 to give the cationic bimetallic complexes, [Fe(CO)2(LMo or LW)(Cp or Cp′)]I (15–18). The cationic nature of these complexes was established by reacting equimolar amounts of [Fe(CO)2LWCp]I with Na[BPh4] in CH2Cl2 to give the anion-exchanged product, [Fe(CO)2LWCp][BPh4] (19)." @default.
• W2000822030 created "2016-06-24" @default.
• W2000822030 creator A5003257162 @default.
• W2000822030 creator A5090525134 @default.
• W2000822030 date "2002-10-01" @default.
• W2000822030 modified "2023-09-30" @default.
• W2000822030 title "The reactions of the monodentate organometallic phosphines [MI2(CO)3{MeC(CH2PPh2)3-P,P′}] (M=Mo, W) with π-allyl molybdenum(II) complexes and iron(O) and iron(II) carbonyl complexes" @default.
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• W2000822030 doi "https://doi.org/10.1016/s0277-5387(02)01164-6" @default.
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