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- W2000832732 abstract "A novel series of [(dpca)MX2] (M = Cu, X = Cl; M = Cd, X = Br and M = Zn, X = NO3) complexes were synthesized through the reaction of N,N-di(2-picolyl)cyclohexylamine (dpca) with the corresponding metal starting materials. X-ray crystallographic analysis determined that the metal center in complexes [(dpca)CuCl2], [(dpca)CdBr2] and [(dpca)Zn(NO3)2] showed a distorted 5-coordinated square pyramidal, trigonal bipyramidal, and 7-coordinated pentagonal bipyramidal geometry, respectively, involving coordination of the nitrogen atom of the cyclohexylamine moiety with the metal center. Specifically, the catalytic activity of [(dpca)Zn(NO3)2] (1.04 × 105 g PMMA/mol Zn·h) for the polymerization of methyl methacrylate (MMA) in the presence of modified methylaluminoxane (MMAO) at 60 °C was six-fold higher than the reference complex [ZnCl2] (1.73 × 104 g PMMA/mol Zn·h)." @default.
- W2000832732 created "2016-06-24" @default.
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- W2000832732 date "2014-07-01" @default.
- W2000832732 modified "2023-09-25" @default.
- W2000832732 title "Synthesis and structural characterization of [(dpca)MX2] (M=Cu, X=Cl; M=Cd, X=Br and M=Zn, X=NO3) complexes containing N,N-di(2-picolyl)cyclohexylamine (dpca) and their application to methyl methacrylate polymerization" @default.
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- W2000832732 doi "https://doi.org/10.1016/j.inoche.2014.04.005" @default.
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