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• W2000841302 abstract "Abstract Electrochemical polymerization of benzene has been carried out in a one-compartment cell using indium-tin oxide conducting glass as a working electrode and Pt mesh as a counterelectrode by the use of a composite electrolyte of aluminum chloride and copper(I) chloride in nitrobenzene. On applying a constant voltage at + 1.8 V vs SCE, a brown and flexible polyparaphenylene (PPP) film was smoothly obtained on the ITO anode surface. The electrical conductivity of the film as grown was 1.9 × 10−5 S/cm. Aluminum and chlorine atoms were detected in the film from XPS studies, so the film might contain AlCl4 − (and Cl−) as a dopant. Scanning electron micrographs of the growing side surface of the film prepared at a constant potential of + 1.8 V vs SCE showed a fibrillar morphology. The fibril diameter (∼100 nm) was similar to that of a polyaniline film. The PPP film exhibited a spin concentration of 1.0 × 1019 spins/g, which corresponds to 800 phenylene units per spin. The g-value and the peak-to-peak lin..." @default.
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• W2000841302 date "1990-08-01" @default.
• W2000841302 modified "2023-10-04" @default.
• W2000841302 title "Electrochemical Polymerization of Benzene by use of Aluminum Chloride and Copper(I) Chloride" @default.
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• W2000841302 doi "https://doi.org/10.1080/00222339009349703" @default.
• W2000841302 hasPublicationYear "1990" @default.
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