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- W2000853025 abstract "The aromatic PCH–N heterocycle 1 with dicoordinated phosphorus (σ2P) reacts with Fe3(CO)12 in toluene or benzene under reductive C–C coupling and coordination of the [Fe2(CO)6]2+ fragment to the μ2-bridging 1,2-bis(phosphido)Fe2(CO)6 chelate complex 2 (rac/meso 4:1 to 2:1). This reaction illustrates the potential of Fe3(CO)12 for C–C coupling reactions of easily reducible unsaturated heterocycles which may act as both, substrate and ligands for coordination of the resulting Fe2(CO)6 fragment. The products were identified by characteristic NMR data of the bis(dihydrobenzazaphospholide) ligands and rac-2·1.5 CDCl3 by crystal structure analysis." @default.
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- W2000853025 date "2015-01-01" @default.
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- W2000853025 title "π-Excess aromatic σ2P ligands: Unprecedented reductive C–C coupling of neopentylbenzazaphosphole at the PCH–N group by Fe3(CO)12 to an heterocyclic 1,2-bis(phosphido)-Fe2(CO)6 complex" @default.
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- W2000853025 doi "https://doi.org/10.1016/j.jorganchem.2014.10.051" @default.
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