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• W2000854414 abstract "The synthesis of a series of trisaminopyridinato metal(III) complexes (metalTi, V and Cr) is reported. The titanium complex is synthesized by reduction of the monochloro TiIV complex (4-Me-TMS-APy)2Ti(NMe2)Cl (4-methyl-2-trimethylsilylaminopyridine = 4-Me-TMS-APyH) using sodium amalgam as a reducing agent. The vanadium complex is prepared via a salt elimination route using VCl3(THF)3 and 3 equiv of in situ lithiated 4-Me-TMS-APyH. The chromium complex is made via benzene elimination from Ph3Cr(THF)3 and 3 equiv of 4-Me-TMS-APyH. All three compounds are paramagnetic and the IR spectra of the compounds fit very well in the finger print range. The X-ray crystal structure analyses of the titanium and the chromium complexes establish their mononuclear structures with a strongly disturbed octahedral coordination geometry. The EPR spectra of the TiIII and CrIII complexes are reported." @default.
• W2000854414 created "2016-06-24" @default.
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• W2000854414 date "1998-03-01" @default.
• W2000854414 modified "2023-09-23" @default.
• W2000854414 title "Homoleptic trisaminopyridinato MIII complexes (MTi, V and Cr), synthesis, structure and EPR investigations" @default.
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• W2000854414 doi "https://doi.org/10.1016/s0277-5387(97)00281-7" @default.
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