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• W2000905441 abstract "Abstract The deposition of Pd nanoparticles on the binary compound Mg 0.65 Sc 0.35 using the Supercritical Fluid Chemical Deposition (SFCD) method was performed. There, the SFCD operating parameters (co-solvent, temperature, CO 2 and hydrogen pressure, reaction time) have been optimized to obtain homogeneous deposition of Pd nanoparticles (around 10 nm). The hydrogenation properties of the optimized Pd@Mg 0.65 Sc 0.35 material were determined and compared to those of Mg 0.65 Sc 0.35 Pd 0.024 . The latter compound forms at 300 °C and 1 MPa of H 2 a hydride that crystallizes in the fluorite structure, absorbs reversibly 1.5 wt.% hydrogen and exhibits fast kinetics. In contrast, Pd@Mg 0.65 Sc 0.35 compound decomposes into ScH 2 and MgH 2 during hydrogen absorption under the same conditions. However, reversible sorption reaches 3.3 wt.% of hydrogen while keeping good kinetics. The possible roles of Pd on the hydrogen-induced alloy decomposition are discussed." @default.
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• W2000905441 date "2013-10-01" @default.
• W2000905441 modified "2023-10-17" @default.
• W2000905441 title "Supercritical fluid chemical deposition of Pd nanoparticles on magnesium–scandium alloy for hydrogen storage" @default.
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• W2000905441 doi "https://doi.org/10.1016/j.jallcom.2013.03.229" @default.
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