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- W2000960083 abstract "39 and 49 cm ‐1 , respectively, from those of BBA. We have undertaken the X-ray analysis of DMABBA in order to clarify the structural features causing the IR frequency changes. N,N-Dimethylaniline was allowed to react with phthalic anhydride in the presence of anhydrous aluminum chloride in carbon disulfide. The reaction mixture was separated by decantation from the solvent and decomposed with diluted sulfuric acid. The insoluble solid was filtered off, and the filtrate was neutralized to pH 2 ‐3 with 10% sodium hydroxide aqueous solution. The crude o-(p-N,N-dimethylaminobenzoyl)benzoic acid was obtained as greenish yellow solid and recrystallized from aqueous ethanol (mp 201.5˚C). A prism with approximate dimensions of 0.36 mm × 0.29 mm × 0.18 mm was mounted on a glass rod. The detailed measurement conditions and crystal data are listed in Table 1. The hydrogen atoms bonded to the C16 atom were assigned based on the expected bonding geometry, and those bonded to the others were found in a difference-Fourier map. The nonhydrogen and the hydrogen atoms were refined anisotropically and isotropically, respectively. The neutral atomic scattering factors were taken from Cromer and Waber. 7 Anomalous" @default.
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- W2000960083 date "2002-03-01" @default.
- W2000960083 modified "2023-09-24" @default.
- W2000960083 title "Crystal Structure of o-(p-N,N-Dimethylaminobenzoyl)benzoic Acid" @default.
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- W2000960083 doi "https://doi.org/10.2116/analsci.18.371" @default.
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