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- W2000993402 abstract "The methanolic extract of saffron was prefractionated with the aid of multilayer coil countercurrent chromatography (MLCCC). After subsequent purification of certain fractions by high-performance liquid chromatography, the following glycoconjugates were isolated and identified on the basis of their spectral (UV, MS, NMR) data: the β-d-glucosides of (4R)-4-hydroxy-3,5,5-trimethylcyclohex-2-enone (5), (4S)-4-hydroxy-3,5,5-trimethylcyclohex-2-enone (6), and (4S)-4-(hydroxymethyl)-3,5,5-trimethylcyclohex-2-enone (7), as well as the β-d-gentiobiosyl ester of 2-methyl-6-oxohepta-2,4-dienoic acid (4). In addition to these new natural products, known saffron constituents, i.e., the di-β-d-gentiobiosyl and β-d-gentiobiosyl-β-d-glucopyranosyl esters of crocetin, have also been isolated and separated using MLCCC. Keywords: (4R)-4-Hydroxy-3,5,5-trimethylcyclohex-2-enone 4-O-β-d-glucopyranoside; (4S)-4-hydroxy-3,5,5-trimethylcyclohex-2-enone 4-O-β-d-glucopyranoside; (4S)-4-(hydroxymethyl)-3,5,5-trimethylcyclohex-2-enone 4-O-β-d-glucopyranoside; β-d-gentiobiosyl ester of 2-methyl-6-oxohepta-2,4-dienoic acid; crocetin derivatives; carotenoid degradation products; multilayer coil countercurrent chromatography; saffron; Crocus sativus; Iridaceae" @default.
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- W2000993402 date "1997-05-01" @default.
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- W2000993402 title "Novel Glycosidic Constituents from Saffron" @default.
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- W2000993402 doi "https://doi.org/10.1021/jf960861k" @default.
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