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- W2001000460 abstract "The photoreduction fluorescence detector functions by monitoring the change in fluorescence accompanying the photoreduction of anthraquinone-2,6-disulfonate to dihydroxyanthracene-2,6-disulfonate by alcohols, aldehydes, ethers, and saccharides. Since the photoreduction of anthraquinone only requires the anthraquinone and not the analyte (alcohol aldehyde, etc.) to absorb light, the detector can be employed to determine compounds which have extremely low UV—visible extinction coefficients. In this paper we present detailed optimization studies on the photochemistry involved in this detection scheme and demonstrate this detector for the determination of cardiac glycosides and common food saccharides in relevant samples. Detection limits for the the cardiac glycosides are in the low picomole range, whereas the saccharides can be determined in the low nanomole range. The detector exhibits a linear response for diginatin in the range 50–500 ng; the reproducibility was calculated to be 6.0% RSD." @default.
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- W2001000460 date "1983-12-01" @default.
- W2001000460 modified "2023-10-10" @default.
- W2001000460 title "Liquid chromatographic detection of cardiac glycosides and saccharides based on the photoreduction of anthraquinone-2,6-disulfonate" @default.
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- W2001000460 doi "https://doi.org/10.1016/s0021-9673(00)91603-0" @default.
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