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- W2001133343 abstract "Four cephalosporins, cefazolin, ceftizoxime, cefaloridine and cefaclor, were determined using a novel microbore high-performance liquid chromatographic system designed to be entirely compatible with direct liquid interfacing (DLI) for mass spectrometric analysis. The chromatographic support was a 5-μm C18 column of 0.3 mm I.D., compared with the usual microbore column diameters of 1–2 mm. The mobile phase contained no buffers or salts which may have caused column blocking or mobile phase crystallization, and the use of a concentration column allowed the injection of large volumes of analyte (up to 500 μl). The assay was reproducible, the relative standard deviations being less than 20% within-day and between-day for all the drugs. The detection limit for cefaloridine and cefazolin was 1 ng and for cefaclor and ceftizoxime 5 ng." @default.
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- W2001133343 date "1991-01-01" @default.
- W2001133343 modified "2023-10-10" @default.
- W2001133343 title "High-performance liquid chromatographic determination of cephalosporin antibiotics using 0.3 mm I.D. columns" @default.
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- W2001133343 doi "https://doi.org/10.1016/s0021-9673(01)95377-4" @default.
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