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- W2001133459 abstract "Abstract The crystal structure of zigrasite, ideally MgZr(PO 4 ) 2 (H 2 O) 4 , a 5.3049(2), b 9.3372(4), c 9.6282(5) Å, α 97.348(1)°, β 91.534(1)°, γ 90.512(4)°, V 472.79(5) Å 3 , Z = 2, triclinic, P 1 , D calc. 2.66 g.cm –3 , from the giant 1972 pocket at Newry, Oxford County, Maine, USA, has been solved and refined to R 1 3.75% on the basis of 2623 unique reflections ( F o > 4σ F ). There are two P sites, each of which is solely occupied by P with <P–O> distances of 1.532 and 1.533 Å, respectively. There are two Mg sites, both of which are occupied by Mg and are octahedrally coordinated two O anions and four (H 2 O) groups with <Mg–O> distances of 2.064 and 2.075 Å, respectively. There is one Zr site, occupied by Zr and octahedrally coordinated by six O anions with a <Zr–O> distance of 2.065 Å . The (ZrO 6 ) octahedron shares corners with six (PO 4 ) tetrahedra, forminga [Zr(PO4) 2 ] sheet parallel to (001). These sheets are stacked in the c direction and linked by (MgO 2 (H 2 O) 4 ) octahedra that share O atoms with the (PO 4 ) groups. The structure is formally a heteropolyhedral framework structure, but the linkage is weaker in the c direction, accounting for the marked (001) cleavage." @default.
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- W2001133459 date "2010-06-01" @default.
- W2001133459 modified "2023-09-26" @default.
- W2001133459 title "The crystal structure of zigrasite, MgZr(PO4)2(H2O)4, a heteropolyhedral framework structure" @default.
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- W2001133459 doi "https://doi.org/10.1180/minmag.2010.074.3.567" @default.
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