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Matches in SemOpenAlex for { <https://semopenalex.org/work/W2001199429> ?p ?o ?g. }

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• W2001199429 abstract "We report a method for the synthesis of N-protected staurosporinones, which are useful for the synthesis of indolo[2,3-a]pyrrolo[3,4-c]carbazole alkaloids and related compounds. An interaction of gramine methiodide (2) with 3-(N-benzyl)indolylacetonitrile (3) in the presence of t-BuLi, followed by a CF3COOH-catalyzed intramolecular indole−indole coupling and dehydrogenation with DDQ, produced 5-cyanoindolo[2,3-a]carbazole 6 almost quantitatively. Reduction of its cyano group followed by N-benzylation produced N-benzylaminomethylindolo[2,3-a]carbazole 8b, which was subjected to Pd(OAc)2-catalyzed direct aromatic carbonylation to give N-protected staurosporinone 9b. Treatment with AlCl3 in anisole removed N-benzyl groups to afford staurosporinone quantitatively." @default.
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• W2001199429 date "2007-02-20" @default.
• W2001199429 modified "2023-09-26" @default.
• W2001199429 title "Synthesis of <i>N</i>-Protected Staurosporinones" @default.
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• W2001199429 doi "https://doi.org/10.1021/jo062184r" @default.
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