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- W2001329721 abstract "Hyperbranched poly(aryl ether ketone)s with hydroxyl end groups (HBP‐OH) and high degree of branching value (83%) were synthesized via an A 2 + B 3 approach. The polymerization conditions (e.g., polymerization temperature and time, monomer concentration, stoichiometric ratio of functional groups) were explored to avoid the gelation. Allyl‐terminated hyperbranched PAEKs (HBP‐AL) with low molecular weight ( M n = 3.4 × 10 3 ) and narrow polydispersity (PDI = 1.65) were obtained via the etherification of HBP‐OH and it has been used for the modification of bismaleimide (BMI) resins. The prepolymers showed good processibilities with a viscosity below 0.6 Pa s at 110°C, though the viscosities slightly increased as the increase of HBP‐AL contents. The cured BMI resins showed high glass transition temperatures ( T g > 320°C) and good thermal stabilities ( T d > 400°C, both in nitrogen and air). It is inspiring to note that the incorporation of HBP‐AL into BMI matrix results in a significant enhancement of toughness without any noticeable loss in modulus, processibility, and T g . POLYM. ENG. SCI., 54:1675–1685, 2014. © 2013 Society of Plastics Engineers" @default.
- W2001329721 created "2016-06-24" @default.
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- W2001329721 date "2013-08-05" @default.
- W2001329721 modified "2023-10-06" @default.
- W2001329721 title "One-pot synthesis of hyperbranched poly(aryl ether ketone)s for the modification of bismaleimide resins" @default.
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- W2001329721 doi "https://doi.org/10.1002/pen.23715" @default.
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