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- W2001386768 abstract "To obtain polymer-modified silica (550 nm diameter), trimethoxysilyl-terminated poly(glycidyl methacrylate-co-methyl methacrylate) with epoxy ring (to prevent the formation of carboxyl group) was successfully synthesized. Then, the cross-linking of the grafted copolymer on silica was made using ethylenediamine or hexamethylenediamine of varying alkyl chain lengths, and the stability of cross-linked silica particles was investigated in alkaline aqueous solution. Cross-linked polymer-modified silica based on diamines exhibited much lower reduction rate (in wt %) of the attached polymer to silica than uncross-linked polymer-modified silica. In particular, cross-linked silica composites by ethylenediamine had more stability than cross-linked silica composites by hexamethylenediamine. Finally, the cross-linking reaction of grafted-polymer on silica particles by diamines was confirmed by the 13C CP/MAS NMR spectra measured on polymer-modified silica composites." @default.
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- W2001386768 date "2007-08-07" @default.
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- W2001386768 title "Cross-linking of Grafted Copolymer on Colloidal Silica and Introduction of Surface Amino Group" @default.
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- W2001386768 doi "https://doi.org/10.1295/polymj.pj2007053" @default.
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