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- W2001437011 abstract "Abstract I) A new synthesis of 4′ ‐methyl‐1,2‐benzanthracene (XII) starting from 1‐naphthaldehyde, is described. This synthesis involves the following steps: bromination (5‐bromo‐1‐naphthaldehyde), Wolff‐Kischner reduction (5‐bromo‐1‐methylnaphthalene), Grignard condensation with phthalic anhydride (5′‐methyl‐α‐naphthoyl‐o‐benzoic acid), cyclisation (4′‐methyl‐1,2‐benzanthraquinone), reduction (4′‐methyl‐1,2‐benzanthracene). II) 4′9,10‐ trimethyl ‐1,2‐ benzanthracene (III) has been prepared: a) By a Grignard reaction between methyl‐magnesium iodide and 4′‐methyl‐1,2‐benzanthraquinone (see above) by the method of Sandin and Fieser. b) starting from 1,2‐benzanthraquinone by the following steps: bromination (4′‐bromo‐1,2‐benzanthraquinone), Grignard condensation with methyl‐magnesium iodide (4′‐bromo‐9,10‐dimethyl‐1,2‐benzanthracene) treatment with C 4 H 9 Li and (CH 3 ) 2 SO 4 (4′, 9, 10‐trimethyl‐1,2‐benzanthracene)." @default.
- W2001437011 created "2016-06-24" @default.
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- W2001437011 date "1952-01-01" @default.
- W2001437011 modified "2023-09-27" @default.
- W2001437011 title "Synthèses dans le domaine des hydrocarbures cancérigènes V. 4′méthyl-et 4′,9,10-triméthyl-1,2-benzanthracènes" @default.
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- W2001437011 doi "https://doi.org/10.1002/bscb.19520610504" @default.
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