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- W2001556783 abstract "The Czochralski technique as applied to synthesis of single-crystal proustite Ag3AsS3, pyrargyrite Ag3SbS3, and related compounds is described. Nucleation of the crystal was accomplished by a cold-finger technique using an iridium rod. The melt was covered with a disk to decrease evaporation losses and to segregate the chemically-formed dross from the liquid-solid interface. In addition, a non-stoichiometric variation of composition, involving excesses of the more volatile components, was used to lengthen the life of the melt. Crystals were pulled as fast as 75 mm/hour but best quality material, i.e. material without cellular structure, was obtained using growth rates of approximately 2 mm/hr. Ingots as large as 2.4 cm in diameter were grown without core effects at slow pulling rates. Initial experiments indicated a strong tendency for the heaxagonal crystal to grow in the c-direction, with a lesser preference for 60° orientation. Large single crystals of good quality were obtained and optical properties were investigated in the spectral range 0.5 to 25 μm on X-cut and Z-cut plates. Proustite crystals with resistivities of approximately 108 Ω-cm were obtained." @default.
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- W2001556783 date "1968-01-01" @default.
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- W2001556783 title "Czochralski-grown proustite and related compounds" @default.
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- W2001556783 doi "https://doi.org/10.1016/0022-0248(68)90148-6" @default.
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