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- W2001578312 abstract "The crystalline structures of α-Si3N4 and β-Si3N4 made from rice husk were obtained at room temperature (300 K) from X-ray powder diffraction with CuKα radiation using Rietveld analysis for the two phase mixture. For α-Si3N4 at 300 K, crystal data: Mr = 140.285, the rhombohedral system, P31c, a = 7.7650(4) Å, c = 5.6275(2) Å, V = 293.85(2) Å3, Z = 4, Dx = 3.1709 g cm−3, μ = 133.474 cm−1 (λ = 1.5406 Å), F(000) = 280.0, the structure was refined with 29 parameters to Rb = 2.42%, Rf = 1.78% for 243 peaks. For β-Si3N4 at 300 K, crystal data: Mr = 140.285, the hexagonal system, P63/m, a = 7.6093(8) Å, c = 2.9079(2) Å, V = 145.81(2) Å3, Z = 2, Dx = 3.1951 g cm−3, μ = 134.492 cm−1 (λ = 1.5406 Å), F(000) = 140.0, the structure was refined with 17 parameters to Rb = 3.02%, Rf = 1.88% for 145 peaks. The whole diffraction was fitted and refined with 46 parameters to Rwp = 6.98%, Rp = 5.33% for 3301 step intensities and ‘goodness of fit’ S = 3.50." @default.
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- W2001578312 date "1995-01-01" @default.
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- W2001578312 title "Two phase refinements of the structures of α-Si3N4 and β-Si3N4 made from rice husk by Rietveld analysis" @default.
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- W2001578312 doi "https://doi.org/10.1016/0272-8842(95)95885-l" @default.
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