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- W2001644889 abstract "Eine Synthese des 7,8-Didehydrodesmosterols (18), ausgehend von 22-Hydroxy-23,24-dinorchol-4-en-3-on (1) wird beschrieben. In der 16stufigen Sequenz treten die Zwischenprodukte 2–11 und 14–17 auf. Das Phosphor-ylid 13 spielt dabei als neues Homologisierungsreagens für Carbonylverbindungen in der Abschlußphase der Synthese (11 → 14 → → 17) eine wichtige Rolle. Synthesis of 7,8-Didehydrodesmosterol The synthesis of 7,8-didehydrodesmosterol (18) starting from 22-hydroxy-23,24-dinorchol-4-en-3-one (1) is reported. Compounds 2–11 and 14–17 are intermediates of a 16-step sequence. The ylide 13 – a new reagent for the homologisation of carbonyl compounds – plays an important part in the final steps of the synthesis." @default.
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- W2001644889 date "1983-06-15" @default.
- W2001644889 modified "2023-09-26" @default.
- W2001644889 title "Synthese des 7,8-Didehydrodesmosterols" @default.
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- W2001644889 doi "https://doi.org/10.1002/jlac.198319830615" @default.
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