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• W2001746593 abstract "In situ hard X-ray absorption spectroscopy (XAS) at metal K-edges and soft XAS at O K-edge and metal L-edges have been carried out during the first charging process for the layered Li1-xCo1/3Ni1/3Mn1/3O2 cathode material. The metal K-edge XANES results show that the major charge compensation at the metal site during Li-ion deintercalation is achieved by the oxidation of Ni2+ ions, while the manganese ions and the cobalt ions remain mostly unchanged in the Mn4+ and Co3+ state. These conclusions are in good agreement with the results of the metal K-edge EXAFS data. Metal L-edge XAS results at different charge states in both the FY and PEY modes show that, unlike Mn and Co ions, Ni ions at the surface are oxidized to Ni3+ during charge, whereas Ni ions in the bulk are further oxidized to Ni4+ during charge. From the observation of O K-edge XAS results, we can conclude that a large portion of the charge compensation during Li-ion deintercalation is achieved in the oxygen site. By comparison to our earlier results on the Li1-xNi0.5Mn0.5O2 system, we attribute the active participation of oxygen in the redox process in Li1-xCo1/3Ni1/3Mn1/3O2 to be related to the presence of Co in this system." @default.
• W2001746593 created "2016-06-24" @default.
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• W2001746593 date "2005-11-18" @default.
• W2001746593 modified "2023-10-13" @default.
• W2001746593 title "Investigation of the Charge Compensation Mechanism on the Electrochemically Li-Ion Deintercalated Li₁_-<i>_x</i>Co_1/3Ni_1/3Mn_1/3O₂ Electrode System by Combination of Soft and Hard X-ray Absorption Spectroscopy" @default.
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• W2001746593 doi "https://doi.org/10.1021/ja0530568" @default.
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