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- W2001940429 abstract "Abstract The heterobimetallic complex, [Et 4 N][W(CO) 5 OPh(Cr(CO) 3 )] ( 1 ), was prepared by the reaction of [Et 4 N][W(CO) 5 CH 3 ] and (η 6 C 6 H 5 OH)Cr(CO) 3 in tetrahydrofuran. Complex 1 crystallizes from THF/hexane in the space group P 2 1 with unit cell dimensions a = 7.036(2) A, b = 11.766(4) A, c = 15.460(4) A, β = 94.83(2)°, V = 1275.3(7) A 3 , and D calcd = 1.779 g cm −3 . The structure was refined to R = 0.084 and R w = 0.091 for 1136 reflections having F > 3.0σ( F o ). Complex 1 was completely inert towards carbon dioxide, even at high pressure (900 psi), but readily reacted with carbonyl sulfide to afford the thiocarbonate derivative, [Et 4 N][W(CO) 5 SC(O)OPh(Cr(CO) 3 )]." @default.
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- W2001940429 date "1993-06-01" @default.
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- W2001940429 title "The synthesis and X-ray structure of a phenoxide-bridged heterobimetallic anion, W(CO)5OPh(Cr(CO)3) −, and its reactivity with carbon dioxide and carbonyl sulfide" @default.
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- W2001940429 doi "https://doi.org/10.1016/0022-328x(93)83011-j" @default.
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