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- W2002024182 abstract "Various alkanedithiols [HSRSH; R = (CH2)3–6 orCH2CH2OCH2CH2] add to the carbon-carbon double bonds of N,N′-bismaleimido-1,8-octane (1) at room temperature in m-cresol that contains triethylamine as a catalyst to produce the corresponding polyimidosulfides (3) in yields of 75–86% and with inherent viscosities (ηinh) of 0.30–1.05 dL/g. In general (3) are amorphous, elastomeric materials that undergo glass transitions (Tg) within the range of 6.5–13°C but product (3a) [R = (CH2)6] is a tough, leatherlike polymer that exhibits Tg = 35°C and a melting transition at 77°C. X-ray analysis indicates that (3a) is ca. 37% crystalline. In addition to further details of the synthesis and properties of polyimidosulfides (3), comparisons are made between crystalline (3a) and a structurally analogous but morphologically dissimilar, elastomeric polyaspartimide synthesized earlier1 J. E. White, M. D. Scaia, and D. A. Snider, J. Appl. Polym. Sci., in press. from (1) and N,N′-dimethyl-1,6-hexanediamine." @default.
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- W2002024182 date "1984-03-01" @default.
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- W2002024182 title "Synthesis and properties of some new polyimidosulfides with highly mobile backbones" @default.
- W2002024182 doi "https://doi.org/10.1002/pol.1984.170220308" @default.
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