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- W2002092007 abstract "Benzyliden-aceton-oxim wurde als Natriumsalz mit Dialkylaminoathylchloriden zu den Oximinoathern umgesetzt. Diese liesen sich auch aus dem Keton und den O-Alkylhydroxylaminen synthetisieren, welche durch hydrolytische Spaltung der O-Alkyl-aceton-oxime zu erhalten waren. Im NMR-Spektrum zeigten die substituierten Aceton-oxime im Gegensatz zum Grundkorper eine Aufspaltung des Methylsignals; die O-Alkyl-benzyliden-aceton-oxime lagen praktisch als reine E-Formen vor; bei der Umsetzung zwischen Benzyliden-aceton-oxim und 2-Chlor-1-dimethyl-amino-propan konnten zwei Umsetzungsprodukte gefunden, getrennt und identifiziert werden.Basic Substituted Styrylalkyl-oximes4-Phenyl-3-buten-2-one-oxime sodium reacted with dialkylaminoalkyl chlorides to the oximino ethers. These were also prepared from the ketone and O-alkylated hydroxylamines, which could be synthesised by hydrolysis of O-alkyl acetone oximes. All substances were examined by nmr-spectroscopy: the substituted acetone oximes showed two signals of the methyl groups contrary to acetone oxime itself; the O-alkylated oximes were almost pure E-isomers, and in the reaction between 4-phenyl-3-buten-2-one-oxime sodium and 2-chloro-1-dimethylamino-propane two products were found, separated, and identified." @default.
- W2002092007 created "2016-06-24" @default.
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- W2002092007 date "1971-01-01" @default.
- W2002092007 modified "2023-09-25" @default.
- W2002092007 title "Basisch substituierte Styrylalkyloxime. Mitt. über ungesättigte Oxime" @default.
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- W2002092007 doi "https://doi.org/10.1002/ardp.19713040613" @default.
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- W2002092007 hasPublicationYear "1971" @default.
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