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• W2002111310 abstract "A pentadentate Schiff base, 2,2′-(((azanediylbis(propane-3,1-diyl))bis(azanylylidene))bis(methanylylidene))diphenol (1), has been synthesized via the reaction of salicylaldehyde with N1-(3-aminopropyl)propane-1,3-diamine [HN(C3H6NH2)2] in absolute ethanol. Refluxing a mixture of 1 with the hydrated acetate salts of nickel(II), zinc(II), iron(II), and copper(II) affords each of the expected M(II)–Schiff base complexes. These complexes have been characterized by means of FT-IR, 1H NMR, 13C NMR, and mass spectrometry as well as UV–Vis spectrophotometry and elemental analysis. In addition, the molecular structures of the copper(II) and nickel(II) complexes were determined by means of X-ray crystallography. Antioxidant and antibacterial activities of 1 and its complexes were evaluated in vitro. Highest DPPH radical-scavenging activity was observed for Fe(II)-1 with an IC50 of 0.39 mg mL−1, followed by 1 (IC50 = 3.38 ± 0.01 mg mL−1). Use of the β-carotene–linoleic acid bleaching assay revealed that 1 has the highest antioxidant activity and has significant inhibition of lipid peroxidation with I% of 94.21 ± 0.003%, followed by Fe(II)-1 and Ni(II)-1 with I% of 34.29 ± 2.08% and 30.77 ± 1.91%, respectively. Antibacterial activity of 1 and its transition-metal complexes was investigated by use of disk diffusion assay; Zn(II)-1 and Ni(II)-1 exert a high inhibition of the growth of all bacterial strains with inhibition diameters ranging from 8 to 14 mm." @default.
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• W2002111310 date "2015-01-01" @default.
• W2002111310 modified "2023-09-27" @default.
• W2002111310 title "Synthesis, characterization, X-ray structures, and biological activity of some metal complexes of the Schiff base 2,2′-(((azanediylbis(propane-3,1-diyl))bis(azanylylidene))bis(methanylylidene))diphenol" @default.
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• W2002111310 doi "https://doi.org/10.1016/j.poly.2014.09.006" @default.
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