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- W2002163544 abstract "Electroreduction of Se(+4) and electrooxidation of Se(−2) were studied at mercury electrodes in acidic media and an improved mechanism of the reduction process was proposed. This mechanism takes into account the fact that the reduction path is concentration-dependent. At lower concentrations of Se(+4), mercury selenide and hydrogen selenide are formed at various potentials. At higher Se(+4) concentrations the electrode quickly becomes covered by a rigid deposit of mercury selenide and then the reduction starts to proceed to elemental selenium. Another form of selenium was formed in the vicinity of the mercury surface due to a chemical reaction between H2SeO3 and H2Se. Oxidation of hydrogen selenide proceeds similarly, in the sense that after coverage of the electrode surface by a deposit of mercury selenide the oxidation starts to proceed to elemental selenium. The cathodic stripping peak of mercury selenide can be obtained down to 2 × 10−8M of Se(+4), but this peak is often split and therefore the determination of traces of Se(+4) by the cathodic stripping technique is cumbersome." @default.
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- W2002163544 date "1982-07-01" @default.
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- W2002163544 title "Cyclic and stripping voltammetry of Se(+4) and Se(−2) at the HMDE in acidic media" @default.
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- W2002163544 doi "https://doi.org/10.1016/0022-0728(82)80040-5" @default.
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