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• W2002191909 abstract "Three new 11β-hydroxy C20 gibberellins have been isolated from immature loquat fruit and their structures were established as 11β-hydroxy-GA12, 11β-hydroxy-GA15 and 11β-hydroxy-GA53, respectively, by direct GC–MS comparisons with authentic samples obtained from gibberellic acid by multistep syntheses. An advanced intermediate (30) was prepared in 20 steps from which 6 11β-hydroxy C20 gibberellins were prepared by parallel routes involving up to a further 5 steps for each sequence. The key steps involved a much improved synthesis of gibberellenic acid derivatives, a Lewis acid catalysed cyclisation of a diazoketone, a domino-hydroboration of a diene and oxidative cleavage of a ketone derived enolate." @default.
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• W2002191909 date "2008-05-01" @default.
• W2002191909 modified "2023-10-09" @default.
• W2002191909 title "Confirmation of structure and synthesis of three new 11β-OH C20 gibberellins from loquat fruit" @default.
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• W2002191909 doi "https://doi.org/10.1016/j.tet.2008.01.131" @default.
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