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- W2002207809 abstract "The macrotricyclic ligand C32H64N4O10 forms with sodium iodide the 1:2 complex of the [3]-cryptate type, (Na2⊂L)I2 (L = C32H64N4O10). This compound crystallizes in space group P21/c with a = 8.726(4), b = 10.114(7), c = 24.422(11)Å, β = 103.89(4)°, Z = 2. The structure was determined from diffractometer data by the heavy atom method and refined by least-squares to R(F) = 0.057 for 1927 reflections. The structure consists of centrosymmetric cations (Na2⊂L)2+ and I− anions; the sodium ions are accommodated inside the tricyclic ligand, with each bonded to two nitrogen and five oxygen atoms of L. The NaN distances are 2.70(1) and 2.73(1) and the NaO range from 2.39(1) to 2.48(1)Å. The iodide ions no longer interact with the sodium ions: all the Na+⋯I− separations exceed 5 Å. The distance between the sodium ions inside L is 6.40 Å." @default.
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- W2002207809 date "1977-01-01" @default.
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- W2002207809 title "Cryptates with macrotricyclic ligands. The structure of the sodium [3]-cryptate [(C32H64N4O10)Na2]I2" @default.
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- W2002207809 doi "https://doi.org/10.1016/s0020-1693(00)86271-4" @default.
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