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- W2002223229 abstract "A gas Chromatographie method is described for the quantitative determination of urinary normetadrenaline, metadrenaline and 3-methoxytyramine using electron capture detection. The N,O-dipentafluoropropionyl (β-O-ethyl derivatives of normetadrenaline and metadrenaline and the N,O-dipentafluoropropionyl derivative of 3-methoxytyramine were prepared. The amines were purified by ion exchange chromatography and ion pair extraction. Amine derivatives from urine extracts were identified definitively by mass fragmentography. The 24-h excretion value for normetadrenaline in human urine is 167 ± 95 μg (mean ± S.D.), for metadrenaline is 116 ± 74 μg (mean ± S.D.) and for 3-methoxytyramine is 82 ± 68 μg (mean ± S.D.)." @default.
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- W2002223229 date "1979-03-01" @default.
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- W2002223229 title "An improved method for the differential assay of 3-omethylated catecholamines in human urine using ion-pair extraction and gas chromatography electron capture detection" @default.
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- W2002223229 doi "https://doi.org/10.1016/0009-8981(79)90118-9" @default.
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