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- W2002249945 abstract "A liquid chromatographic method is described for the determination of daunorubicin using octyldecylsilyl columns and sodium dodecyl sulphate as ion-pairing agent. The method based on a previous publication [M. A. van Lancker et. al., J. Chromatogr., 254 (1983) 45] is specific daunoribicin and separates it from likely impurities, e.g., the aglycone, duborimycin and related anthracyclines,doxurubicin and epirubicin. Several commercial batches have been examined in a number of laboratories employing various types of stationary phases. The intralaboratory reproducibilities varied from 1.0 to 1.6% and teh interlaboratory reproducibility between 0.63 adn 1.0% (based on the means of duplicate determinations), while with the preferred mobile phase the coefficient of variation was 0.3% (n = 4). The method is robust and is proposed for inclusion in a monograph on daunorubicin which is currently under consideration by the European Pharmacopoeia." @default.
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- W2002249945 date "1987-01-01" @default.
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- W2002249945 title "Development of a reversed-phase ion-pairing liquid chromatographic assay of daunorubicin for pharmacopoeial use" @default.
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- W2002249945 doi "https://doi.org/10.1016/s0021-9673(01)94279-7" @default.
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