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- W2002302122 abstract "Silver-ion HPLC (Ag-HPLC) has been utilized to separate a variety of unsaturated fatty acid methyl esters (FAMEs) by configuration, location or number of olefinic or acetylenic bonds. Two analytical Ag-HPLC columns connected in series and an isocratic solvent system of acetonitrile (ACN) in hexane were used to fractionate 10–15 mg samples of a mixture of two deuterium-labeled isomers of conjugated linoleic acid (Z9,E11- and Z9,Z11-octadecadienoic acid-17,17,18,18-d4). “Baseline” (>95%) resolution of the two isomers, which decreased with increasing weights of sample injected, was maintained by careful adjustment of the percentage of ACN in the ACN/hexane solvent system. Chemical purities of the isolated FAME were >96%." @default.
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- W2002302122 date "2004-04-01" @default.
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- W2002302122 title "Separation of conjugated linoleic acid methyl esters by silver-ion high performance liquid chromatography in semi-preparative mode" @default.
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- W2002302122 doi "https://doi.org/10.1016/j.chroma.2003.01.001" @default.
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