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• W2002672007 abstract "Abstract The reaction of (dpp‐bian)Na(Et 2 O) with one equiv. of i PrMgCl in hexane affords (dpp‐bian)Mg‐ i Pr(Et 2 O) ( 1 ) whereas (dpp‐bian)Mg(Et 2 O) 2 ( 2 ) is formed when this reaction is carried out in Et 2 O as a result of isopropyl radical elimination. Compound 1 which is stable in hexane and Et 2 O also decomposes in THF with elimination of isopropyl radicals yielding (dpp‐bian)Mg(THF) 2 . The reaction of (dpp‐bian)Na 2 (Et 2 O) 3 with two equiv. of i PrMgCl in Et 2 O produces 2 and i Pr 2 Mg, which then interact to give (dpp‐bian)(Mg‐ i Pr) 2 (Et 2 O) ( 3 ) when treated with hexane or toluene. Compounds 1 – 3 were characterized by elemental analysis, UV/Vis and NMR spectroscopy, as well as by single‐crystal X‐ray diffraction. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2005)" @default.
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• W2002672007 date "2005-04-01" @default.
• W2002672007 modified "2023-10-01" @default.
• W2002672007 title "Reductive Isopropyl Radical Elimination from (dpp‐bian)Mg‐<i>i</i>Pr(Et₂O)" @default.
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• W2002672007 doi "https://doi.org/10.1002/ejic.200400973" @default.
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