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- W2002776829 abstract "A reversed-phase high-performance liquid chromatographic method, with ultraviolet detection, is proposed for the plasma determination of SIN-1, the active metabolite of molsidomine, which involves propoxycarbonyl derivatization. The internal standard is the ethoxycarbonyl derivative of SIN-1 (i.e. molsidomine). Derivatization and extraction are each performed in one step (2 min) with 70% yield. The nature of a by-product is discussed. The method provides rapid elution (less than 15 min), linearity over the range 0.4–200 ng/ml, day-to-day precision between 2.5 and 11.3% and a limit of determination of 0.5 ng/ml. This method is also suitable for the simultaneous determination of molsidomine and SIN-1. In this case the internal standard is an ethoxycarbonyl derivative of a piperazino-3-sydnonimine, a SIN-1 analogue." @default.
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- W2002776829 date "1990-01-01" @default.
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- W2002776829 title "Determination of the active metabolite of molsidomine in human plasma by reversed-phase high-performance liquid chromatography" @default.
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- W2002776829 doi "https://doi.org/10.1016/s0378-4347(00)82401-9" @default.
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