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- W2003100770 abstract "Abstract Two new ligands, ( S )-Ph 2 POCH 2 CH(NMe 2 )CH 2 CH 2 SCH 3 , derived from L -methionine, and ( R )-Ph 2 POCH 2 CH(NMe 2 )CH 2 -SCH 3 from L-cysteine have been prepared and characterized. Several metal complexes of Pd, Mo and W have been prepared. These ligands produce a chiral electronically asymmetric environment at the metal that is evidenced by trans influences on the other ligands. A crystal structure has been determined for [( S )-Ph 2 POCH 2 CH(NMe 2 )CH 2 CH 2 SCH 3 ]W(CO) 3 . The sulfur adopts an S s configuration in the solid and significant trans influences are observed in the metrical parameters of the carbonyls. This tungsten complex crystallizes in the monoclinic space group P 2 1 with a = 8.8435(6) A, b = 14.384(1) A, c = 9.546(1) A, β = 107.01(8), Z = 2 and V = 1161.0(4) A 3 ." @default.
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- W2003100770 date "1994-04-01" @default.
- W2003100770 modified "2023-09-23" @default.
- W2003100770 title "Metal complexes of new chiral tridentate ligands with N, P and S donors: The crystal structure of [(S)-Ph2POCH2CH(NMe2)CH2CH2SCH3]W(CO)3" @default.
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- W2003100770 doi "https://doi.org/10.1016/0022-328x(94)80047-2" @default.
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