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- W200311 abstract "Core cross-linked star (CCS) polymers prepared from a glycol acrylate core with polystyrene (PS) or poly(methyl methacrylate) (PMMA) branches were added as filler to linear PS or PMMA, respectively. The materials were analysed using modulated temperature thermomechanometry to examine the influence of hyperbranching on structure, morphology and relaxation properties. Isothermal annealing was performed below the onset of the glass transition temperature (Tg) at logarithmically spaced time intervals (1, 10, 100 h) to observe the contribution of physical ageing to structural relaxation. Thermal expansion, shrinkage and the glass transition temperature increased with annealing time, due to reduced free volume and mobility constraining molecular rearrangement. Volume relaxation during isothermal annealing was interpreted using the stretched-exponential function of Kohlrausch, Williams and Watts. (KWW). The experimental and calculated KWW results also support the general concept that structural relaxation is both non-linear and non-exponential." @default.
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- W200311 date "2010-01-01" @default.
- W200311 modified "2023-09-24" @default.
- W200311 title "Thermal ageing and relaxation of core-crosslinked star containing composites using modulated temperature-thermomechanometry" @default.
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