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• W2003111245 abstract "Adsorption−desorption induced structural changes of Cu(bpy)(H2O)2(BF4),(bpy) (bpy = 4,4′-bipyridine) [Cu-MOF] have been evidenced by combined NMR and EPR spectroscopy. Upon adsorption of probe molecules even at a few mbar, EPR spectra show that they are activated to form complexes at Cu(II) sites, which results in a change of the Cu-MOF’s structure as indicated by a high-field shift of the 11B MAS NMR. After desorption, both EPR and 11B MAS NMR spectra evidenced that the structure of the Cu-MOF reversibly shifted to the original state. This observation indicates that MOFs can undergo structural changes during processes where adsorption−desorption steps are involved such as gas storage, separation, and catalysis." @default.
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• W2003111245 date "2009-01-21" @default.
• W2003111245 modified "2023-10-01" @default.
• W2003111245 title "Adsorption−Desorption Induced Structural Changes of Cu-MOF Evidenced by Solid State NMR and EPR Spectroscopy" @default.
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• W2003111245 doi "https://doi.org/10.1021/ja8088718" @default.
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